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자료유형
학술저널
저자정보
안지현 (Korea Polytechnic University) 김병주 (Korea Polytechnic University) 김재근 (Korea Polytechnic University) 김호진 (Korea Polytechnic University) 홍계원 (Korea Polytechnic University) 이희균 (Korea Polytechnic University) 유재무 (Korea Institute of Machinery and Materials)
저널정보
한국초전도학회 Progress in superconductivity Progress in superconductivity 제7권 제1호
발행연도
2005.1
수록면
58 - 63 (6page)

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초록· 키워드

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We investigated the surface oxidation behavior of cube-textured polycrystalline nickel at various oxidation conditions. Cube-textured NiO film was formed on a cube-textured polycrystalline nickel regardless of oxidation conditions but different growth behavior of NiO crystals was observed depending on the oxidation conditions. The introduction of water vapor into $O_2$ did not affect the texture evolution, but rough and porous microstructure was developed. Microstructure of NiO film tends to be denser as the oxygen partial pressure increases. It is interesting that (111) peak of theta - two theta diffraction pattern started to get stronger in air atmosphere and (111) plane became the major texture in the substrate oxidized in high purity argon gas. Small amount of high index crystallographic plane NiO peak crystal was observed when $N_{2}O$ was used as an oxidant while only (200) plane crystal was formed in dry $O_2$ atmosphere. Flat and smooth surface was changed into rough faceted one when ramping rate to oxidation temperature was faster. The grain size of NiO was decreased when the oxygen partial pressure was low. It was also observed that the modification of nickel surface suppressed the development of (200) texture.

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