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학술연구/단체지원/교육 등 연구자 활동을 지속하도록 DBpia가 지원하고 있어요.
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연구자들이 자신의 연구와 전문성을 널리 알리고, 새로운 협력의 기회를 만들 수 있는 네트워킹 공간이에요.
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Sample preparation is very important for crystal structure analysis of novel nano-structured materials in electron microscopy. Generally, a grid dispersion method has been used as transmission electron microscope (TEM) sampling method of nano-powder samples. However, it is diff cult to obtain the cross-sectional information for the tabular-structured materials. In order to solve this problem, we have attempted a new sample preparation method using focused ion beam. Base on this approach, it was possible to successfully obtain the electron diffraction patterns and high-resolution TEM images of the cross-section of tabular structure. Finally, we were able to obtain three-dimensional crystallographic information of novel zeolite nano-crystal of the tabular morphology by applying the new sample preparation technique.
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등록된 정보가 없습니다.
참고문헌 (10)
참고문헌 신청
Chen Y / 2011 / Ultrahigh throughput silicon nanomanufacturing by simultaneous reactive ion synthesis and etching / ACS Nano 5 : 8002 ~ 8012
Corma A / 1995 / Inorganic solid acids and their use in acid-catalyzed hydrocarbon reactions / Chem. Rev 95 : 559 ~ 614
Ferrando-Villalba P / 2014 / In-plane thermal conductivity of sub-20nm thick suspended mono-crystalline Si layers / Nanotechnology 25 : 185402 ~
Jun Y W / 2005 / Symmetry-controlled colloidal nanocrystals: nonhydrolytic chemical synthesis and shape determining parameters / J. Phys. Chem. B 109 : 14795 ~ 14806
Kim J G / 2010 / Structure analysis of inorganic crystals by energy-fi ltered precession electron diffraction / J. Electron Microsc 59 : 273 ~ 283
Corma A / 1995 / Inorganic solid acids and their use in acid-catalyzed hydrocarbon reactions / Chem. Rev 95 : 559 ~ 614
Ferrando-Villalba P / 2014 / In-plane thermal conductivity of sub-20nm thick suspended mono-crystalline Si layers / Nanotechnology 25 : 185402 ~
Jun Y W / 2005 / Symmetry-controlled colloidal nanocrystals: nonhydrolytic chemical synthesis and shape determining parameters / J. Phys. Chem. B 109 : 14795 ~ 14806
Kim J G / 2010 / Structure analysis of inorganic crystals by energy-fi ltered precession electron diffraction / J. Electron Microsc 59 : 273 ~ 283
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