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학술연구/단체지원/교육 등 연구자 활동을 지속하도록 DBpia가 지원하고 있어요.
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논문 기본 정보
- 자료유형
- 학술저널
- 저자정보
- 발행연도
- 2019.1
- 수록면
- 258 - 266 (9page)
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초록· 키워드
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Objectives: In this study, blood lead was analyzed using graphite furnace atomic absorption spectrometry (GFAAs) and inductively coupled plasma mass spectrometry (ICP-MS). We tried to examine the difference and consistency of the analytical values and the applicability of the analytical method. Methods: We selected 57 people who agreed to participate in this study. After confirming the linearity of the calibration standard curves in GF-AAs and ICP-MS, the concentrations of lead in quality control material and samples were measured, and the degree of agreement was compared. Results: The detection limit of the ICP-MS was lower than that of GF-AAs. The coefficient of variation of reference materials was shown to be stable in the ICP-MS and GF-AAs. When the correspondence between the two equipments was verified by bias of the analysis values, a concordance was shown, and approximately 98% of the ideal reference lines were present within ±40% of the deflection. Conclusion: GF-AAs showed high sensitivity to single heavy metal analysis, but it took much time and showed higher detection limit than ICP-MS. Therefore, it would be considered necessary to switch to ICP-MS analysis method, considering that the level of lead exposure is gradually decreasing.
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참고문헌 (30)
참고문헌 신청
김효준 / 2009 / 우리나라 일부 도시와 농촌지역 주민의 혈중 납 및 혈중 카드뮴 농도 / 생명과학회지 19(4):472~478
Zhang ZW / 1997 / Background exposure of urban populations to lead and cadmium: comparison between China and Japan / International Archives of Occupational and Environmental Health 69(4):273~281
Lee JS / 2008 / Establishment of analytical method for blood and urine using ICP/MS (I) :1~86
Torrence KM / 2002 / Slurry sampling for the determination of arsenic, cadmium, and lead in mainstream cigarette smoke condensate by graphite furnace–atomic absorption spectrometry and inductively coupled plasma–mass spectrometry / Analytical and Bioanalytical Chemistry 372(5-6):723~731
Trzcinka-Ochocka M / 2016 / Useful and Fast Method for Blood Lead and Cadmium Determination Using ICP-MS and GF-AAS; Validation Parameters / Journal of Clinical Laboratory Analysis 30(2):130~139
Zhang ZW / 1997 / Background exposure of urban populations to lead and cadmium: comparison between China and Japan / International Archives of Occupational and Environmental Health 69(4):273~281
Lee JS / 2008 / Establishment of analytical method for blood and urine using ICP/MS (I) :1~86
Torrence KM / 2002 / Slurry sampling for the determination of arsenic, cadmium, and lead in mainstream cigarette smoke condensate by graphite furnace–atomic absorption spectrometry and inductively coupled plasma–mass spectrometry / Analytical and Bioanalytical Chemistry 372(5-6):723~731
Trzcinka-Ochocka M / 2016 / Useful and Fast Method for Blood Lead and Cadmium Determination Using ICP-MS and GF-AAS; Validation Parameters / Journal of Clinical Laboratory Analysis 30(2):130~139
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