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학술연구/단체지원/교육 등 연구자 활동을 지속하도록 DBpia가 지원하고 있어요.
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논문 기본 정보
- 자료유형
- 학술저널
- 저자정보
- 발행연도
- 2007.1
- 수록면
- 421 - 428 (8page)
이용수
초록· 키워드
오류제보하기
This study was conducted two kinds of aims: 1) to modify the analytical methods(conditions) by high performance liquid chromatography-fluorescence detector for the detection of residual ivermectin in raw milk, 2) to provide basic information for the evaluation of standard of the residual ivermectin in raw milk.It could be considerable that negative ion spectra can be better method in the LC/MS analysis for the detection of residues. Characteristic daughter ions were observed in negative ion spectra, however, linear line was not formed in positive ion one.Three Holstein cows (500±10kg) were applied to commercial ointment of ivermectin just one time at the first day of test, and residues in raw milk were examined for 20day after administration. The limit of detection(LOD) was 0.65ng(n=5) by HPLC/FLD, and recovery rates were 87.85%~99.47%. The peak was observed at the 4th day, and residues lasted to the end. Thus ivermectin was prohibited when lactating.
목차
등록된 정보가 없습니다.
참고문헌 (10)
참고문헌 신청
Codex Alimentarius Commission / 2005 / Maximum residues limits for veteri?nary drug in foods : 1 ~ 25
Danaher M / 2000 / Validation and robustness testing of a HPLC method for the determi?nation of avermectins and moxidectin in animal liver samples using an alu?mina column cl
Durden DA / 2007 / Positive and nega?tive electrospray LC-MS-MS methods for quantitation of the antiparasitic endectocide drugs, abamectin, doramec?tin, emamectin, eprinomect
Howells L / 2001 / residue analysis of avermectins and moxidectin by ion?trap LC?MSn 126 ( ) : 155 ~ 160
Imperiale F / 2004 / Comparative depletion of ivermectin and moxidectin milk resi?dues in dairy sheep after oral and subcutaneous administration 71 : 427 ~ 433
Danaher M / 2000 / Validation and robustness testing of a HPLC method for the determi?nation of avermectins and moxidectin in animal liver samples using an alu?mina column cl
Durden DA / 2007 / Positive and nega?tive electrospray LC-MS-MS methods for quantitation of the antiparasitic endectocide drugs, abamectin, doramec?tin, emamectin, eprinomect
Howells L / 2001 / residue analysis of avermectins and moxidectin by ion?trap LC?MSn 126 ( ) : 155 ~ 160
Imperiale F / 2004 / Comparative depletion of ivermectin and moxidectin milk resi?dues in dairy sheep after oral and subcutaneous administration 71 : 427 ~ 433
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