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논문 기본 정보
- 자료유형
- 학술저널
- 저자정보
- 발행연도
- 2015.1
- 수록면
- 259 - 264 (6page)
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We investigated the residues of 6 cephalosporins (cefquinome, cephalexin, cephalonium, cefazolin, cef-tiofur, cefuroxime) using LC-MS/MS in raw meat in Seoul. This method involves extraction of the resi-due from the meat by distilled water and methanol followed by a manual of residue analysis published by the National Institute of Food and Drug Safety Evaluation. The recoveries ranged between 74.71∼90.01% in beef, 73.37∼101.40% in pork and 70.87∼95.53% in chicken, respectively. The limits of detection were 0.0004∼0.0563 mg/kg, and the limits of quantification were 0.001∼0.169 mg/kg respectively. Residues of cephalosporins which exceeded maximum residue limits (MRL) were not ex-ceed in any of the 287 samples. However, it is necessary to develop multi-method, which includes the active metabolites of ceftiofur.
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참고문헌 (26)
참고문헌 신청
Australian Government department of agriculture / / Animal product monitoring results tables 2013-14 Meat, Poultry Annual Results 2013-2014, Beef Annual Report 2013-2014
Becker M / 2004 / Residue analysis of 15 penicillins and cephalosporins in bovine muscle, kidney and milk by liquid chromatography-tandem mass spectrometry / Analytica Chimi
Berendsen BJ / 2012 / Assessment of liquid chromatography-tandem mass spectrometry approaches for the analysis of ceftiofur metabolites in poultry muscle / Food Addit Contam
Dancer SJ / 2001 / The problem with cephalosporins / J Antimicrob Chemother 48 : 463 ~ 478
FDA / 2012 / CODEX Guideline for validation of Chemical Methods for the FDA Foods Program / Appendix 2 : 25 ~ 26
Becker M / 2004 / Residue analysis of 15 penicillins and cephalosporins in bovine muscle, kidney and milk by liquid chromatography-tandem mass spectrometry / Analytica Chimi
Berendsen BJ / 2012 / Assessment of liquid chromatography-tandem mass spectrometry approaches for the analysis of ceftiofur metabolites in poultry muscle / Food Addit Contam
Dancer SJ / 2001 / The problem with cephalosporins / J Antimicrob Chemother 48 : 463 ~ 478
FDA / 2012 / CODEX Guideline for validation of Chemical Methods for the FDA Foods Program / Appendix 2 : 25 ~ 26
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