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논문 기본 정보
- 자료유형
- 학술저널
- 저자정보
- 발행연도
- 2016.1
- 수록면
- 1 - 6 (6page)
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Phlorotannins are reported to have diverse biological properties. However, no analytical methods for the standardization of phlorotannin preparations have been reported. Herein, we developed and validated an analytical method for the determination of dieckol in phlorotannin extracts (PRT) using high-performance liquid chromatography (HPLC). The optimum HPLC conditions consisted of a Supelco Discovery C18 column stationary phase, a mobile phase (A: 15 % HPLC grade methanol in deionized water, B: methanol), UV detection at 230 nm, and a flow rate of 0.7 mL/min. The optimized chromatographic conditions were validated and exhibited good specificity and linearity (R2 > 0.9994–1.0000). The recoveries were in the range of 100.9–102.3 %. The method had good intermediate (%RSD 1.2) and intra-day (%RSD 0.4–1.7) assay precisions. This HPLC method had good accuracy and quality in the determination of dieckol in PRT.
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참고문헌 (17)
참고문헌 신청
Bai SC / 2015 / Outlook for Korean Aquaculture / Aquainfo 3(1):20~41
FAO / FAO Global Capture Production database updated to 2013 – Summary information
황보영 / 2009 / The Frequency and Length Dependence of the Target Strength of the Largehead Hairtail (Trichiurus lepturus) in Korean Waters / Fisheries and Aquatic Sciences 12(2):152~161
정우건 / 2009 / Studies for the Sustainable Management of Oyster Farms in Pukman Bay, Korea: Estimate of Primary Production / Fisheries and Aquatic Sciences 12(2):111~117
정우건 / 2009 / Studies for the Sustainable Management of Oyster Farms in Pukman Bay, Korea: Estimation of Carrying Capacity from Food Availability / Fisheries and Aquatic Sciences 12(2):118~129
FAO / FAO Global Capture Production database updated to 2013 – Summary information
황보영 / 2009 / The Frequency and Length Dependence of the Target Strength of the Largehead Hairtail (Trichiurus lepturus) in Korean Waters / Fisheries and Aquatic Sciences 12(2):152~161
정우건 / 2009 / Studies for the Sustainable Management of Oyster Farms in Pukman Bay, Korea: Estimate of Primary Production / Fisheries and Aquatic Sciences 12(2):111~117
정우건 / 2009 / Studies for the Sustainable Management of Oyster Farms in Pukman Bay, Korea: Estimation of Carrying Capacity from Food Availability / Fisheries and Aquatic Sciences 12(2):118~129
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