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학술연구/단체지원/교육 등 연구자 활동을 지속하도록 DBpia가 지원하고 있어요.
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In this study, we purified an environmental pollutant (metamifop) by re-crystallization under various conditions and prepared four kinds of high-purity reference materials (RM) that show small variations in purity among each other. To measure their purities with uncertainty, four different analytical methods were employed: differential scanning calorimetry (DSC), peak area normalization (HPLC), external calibrant (HPLC), and quantitative NMR (q-NMR). The highest purity of metamifop RM, determined by q-NMR, was 99.02% with an uncertainty of 0.64% compared with 99.36% (with 0.12% uncertainty), 99.46% (with 0.53% uncertainty) and 99.84% (with 0.29% uncertainty), determined by DSC, external calibrant, and peak area normalization, respectively. Most of the evaluated purities are within the calculated uncertainty range
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참고문헌 (16)
참고문헌 신청
장해성 / 2004 / 2-[4-(6-chloro-2-benzoxazolyloxy)phenoxy]-propionamide 유도체의 합성과 제초 활성 / 농약과학회지 8(2):145~149
X. Xia / 2016 / Mechanism of metamifop inhibition of the carboxyl- transferase domain of acetyl-coenzyme A carboxylase in Echinochloa crus-galli / Scientific Reports 6:34066~34066
S. R. Barik / 2018 / Persistence behavior of metamifop and its metabolite in rice ecosystem / Chemosphere 193:875~882
J. K. Moon / 2010 / Photodegradation Pathways and Mechanisms of the Herbicide Metamifop in a Water/Acetonitrile Solution / J. Agric. Food Chem. 58:12357~12365
H. J. Choi / 2014 / Carcinogenicity of metamifop, a novel herbicide, in Wistar rats following oral administration for 104 weeks / Regulatory Toxicology and Pharmacology 70:535~544
X. Xia / 2016 / Mechanism of metamifop inhibition of the carboxyl- transferase domain of acetyl-coenzyme A carboxylase in Echinochloa crus-galli / Scientific Reports 6:34066~34066
S. R. Barik / 2018 / Persistence behavior of metamifop and its metabolite in rice ecosystem / Chemosphere 193:875~882
J. K. Moon / 2010 / Photodegradation Pathways and Mechanisms of the Herbicide Metamifop in a Water/Acetonitrile Solution / J. Agric. Food Chem. 58:12357~12365
H. J. Choi / 2014 / Carcinogenicity of metamifop, a novel herbicide, in Wistar rats following oral administration for 104 weeks / Regulatory Toxicology and Pharmacology 70:535~544
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