지원사업
학술연구/단체지원/교육 등 연구자 활동을 지속하도록 DBpia가 지원하고 있어요.
커뮤니티
연구자들이 자신의 연구와 전문성을 널리 알리고, 새로운 협력의 기회를 만들 수 있는 네트워킹 공간이에요.
초록· 키워드
오류제보하기
Aluminium (Al) is one of the major elements in rocks and its concentration can be varied, depending on different rock types as well as sources. The present study aimed to propose an analytical method based on the UV-Vis as a cheap, simple, and common instrument equipped in most laboratories for Al quantification in rocks after the microwave assisted acid digestion. The aluminone and 8-hydroxyquinoline were investigated for the colorimetric assay. The results show that the 8-hydroxyquinoline reagent was more favorable in terms of the minimized affects of the potential interferences present in the digested solutions, i.e., Fe<SUP>3+</SUP>, Si<SUP>4+</SUP> and F-. The calibration curve was constructed from 0.10 mg/L to 3.00 mg/L with the goodness of linearity (R² = 0.9996). The limits of detection and quantification (LOD and LOQ) were estimated, i.e., 0.029 mg/L and 0.087 mg/L, respectively. The 8-hydroxyquinoline was applied to real rock samples, demonstrating favorable precision (RSD = 0.34 %-1.8 %) and no remarkable differences were found compared to the inductively coupled plasma-mass spectrometry (ICP-MS) as a reference measurement approach.
목차
Abstract
1. Introduction
2. Experimental
3. Results and Discussion
4. Conclusions
References
참고문헌 (21)
참고문헌 신청
M. Pidwirny, ‘Composition of rocks. Fundamentals of physical geography’, 2nd Ed., Date Viewed, 2006.
S. V. Khromykh, P. D. Kotler, A. V. Kulikova, D. V. Semenova, K. R. Minnebaev, B. I. Gareev, G. A. Batalin, T. N. Antsiferova, E. A. Il’icheva, and A. S. Volosov, Minerals, 12(1), 1-21 (2022).
Z. A. Alhawdar, ‘Method Development for the Analysis of Aluminum, Calcium, Magnesium and Iron in Sedimentary Rocks’ Master Degree Thesis, Pittsburg State University, Pittsburg, Kansas, 2014.
J. A. Haggerty, Geophys. Monogr. Ser., 43, 175-185 (1987).
V. Balaram, R. Mathur, M. Satyanarayanan, S. S. Sawant, P. Roy, K. S. V. Subramanyam, C. T. Kamala, K. V. Anjaiah, S. L. Ramesh, and B. Dasaram, Mapan-J. Metrol. Soc. India, 27, 87-95 (2012).
S. V. Khromykh, P. D. Kotler, A. V. Kulikova, D. V. Semenova, K. R. Minnebaev, B. I. Gareev, G. A. Batalin, T. N. Antsiferova, E. A. Il’icheva, and A. S. Volosov, Minerals, 12(1), 1-21 (2022).
Z. A. Alhawdar, ‘Method Development for the Analysis of Aluminum, Calcium, Magnesium and Iron in Sedimentary Rocks’ Master Degree Thesis, Pittsburg State University, Pittsburg, Kansas, 2014.
J. A. Haggerty, Geophys. Monogr. Ser., 43, 175-185 (1987).
V. Balaram, R. Mathur, M. Satyanarayanan, S. S. Sawant, P. Roy, K. S. V. Subramanyam, C. T. Kamala, K. V. Anjaiah, S. L. Ramesh, and B. Dasaram, Mapan-J. Metrol. Soc. India, 27, 87-95 (2012).
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