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학술연구/단체지원/교육 등 연구자 활동을 지속하도록 DBpia가 지원하고 있어요.
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논문 기본 정보
- 자료유형
- 학술저널
- 저자정보
- 저널정보
- 한국고분자학회 폴리머 폴리머 제45권 제6호
- 발행연도
- 2021.11
- 수록면
- 857 - 864 (8page)
- DOI
- 10.7317/pk.2021.45.6.857
이용수
초록· 키워드
오류제보하기
Interpenetrating polymer networks (IPNs) that have silane resins as one of their components are industrially important due to their physical and chemical properties. The current study included preparation and characterization of two types of unsaturated silane monomers in order to prepare new types of IPNs with unsaturated polyesters (palatal). These monomers were characterized with Fourier transform infrared spectroscopy (FTIR) and nuclear magnetic resonance spectroscopy (<SUP>1</SUP>H NMR), and their molecular weights were determined by cryoscopy technique. The curing properties of the silane monomers and the IPNs were observed by differential scanning calorimetry (DSC), and several of thermal curing functions were determined, such as the initial curing temperature, optimum curing temperature, curing energy, activation energy and rate of curing. There was a significant decrease in the initial and maximum curing temperatures compared with the unsaturated polyester resin (palatal) due to the decrease in the activation energy from 105.4 to 77.3 ºC when the allyoxy silane monomer percentage was shifted from 5 to 20%. Meanwhile, the activation energy for the IPNs based on α-methyl-butenoxy silane decreased from 96.8 to 55.8 kJ/mol.
목차
Abstract
Introduction
Experimental
Results and Discussion
Conclusions
References
참고문헌 (43)
참고문헌 신청
Polymer Blends Handbook; Utracki, L. A., Wilkie, C. A., Eds. Kluwer Academic Publishers: Dordrecht, 2002.
Sperling, L. H.; Mishra, V. B. A. T. The Current Status of Interpenetrating Polymer Networks. Polym. Adv. Technol. 1996, 7, 197-208.
Horák, Z.; Fortelný, I.; Kolařík, J.; Hlavatá, D.; Sikora, A. Polymer Blends. In Encyclopedia of Polymer Science and Technology; John Wiley & Sons: New York, 2005; pp 1-59.
Panteli, P. A.; Patrickios, C. S. Multiply Interpenetrating Polymer Networks: Preparation, Mechanical Properties, and Applications. Gels 2019, 5, 36.
Kamal, M. Camphor and Poly(Antimonyacrylate) Based Interpenetrating Polymer Network: Synthesis and Characterization. Indian J. Chem. Technol. 2011, 18, 284-290.
Sperling, L. H.; Mishra, V. B. A. T. The Current Status of Interpenetrating Polymer Networks. Polym. Adv. Technol. 1996, 7, 197-208.
Horák, Z.; Fortelný, I.; Kolařík, J.; Hlavatá, D.; Sikora, A. Polymer Blends. In Encyclopedia of Polymer Science and Technology; John Wiley & Sons: New York, 2005; pp 1-59.
Panteli, P. A.; Patrickios, C. S. Multiply Interpenetrating Polymer Networks: Preparation, Mechanical Properties, and Applications. Gels 2019, 5, 36.
Kamal, M. Camphor and Poly(Antimonyacrylate) Based Interpenetrating Polymer Network: Synthesis and Characterization. Indian J. Chem. Technol. 2011, 18, 284-290.
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