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논문 기본 정보

자료유형
학술저널
저자정보
Han Sol Lee (National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Ji-Su Park (National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Su Jung Lee (National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Hye-Sun Shin (National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Yun mi Chung (Gwangju Regional Food and Drug Administration) Ha na Choi (Gwangju Regional Food and Drug Administration) Sang Soon Yun (National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Yong-hyun Jung (National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety) Jae-Ho Oh (National Institute of Food and Drug Safety Evaluation, Ministry of Food and Drug Safety)
저널정보
한국분석과학회 분석과학 분석과학 제34권 제1호
발행연도
2021.2
수록면
1 - 8 (8page)

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초록· 키워드

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An analytical method was developed and optimized for the quantification of a plant growth regulator, 2,6-diisopropylnaphthalene (2,6-DIPN), in agricultural products using gas chromatography-tandem mass spectrometry. The samples were extracted, partitioned, and were purified using a Florisil<SUP>®</SUP> cartridge. To validate the analytical method, its specificity, linearity, limit of detection (LOD) and limit of quantification (LOQ) of the instrument, LOQ of the analytical method (MLOQ), accuracy, and repeatability were considered. The method displayed excellent results during validation, and is suitable for the determination and quantification of the low residual levels of the analyte in the agricultural samples. All of the results with the optimized method were satisfactory and within the criteria ranges requested in the Codex Alimentarius Commission guidelines and the Ministry of Food and Drug Safety guidelines for pesticide residue analysis. The developed method is simple and accurate and can be used as a basis for safety management of 2,6-DIPN.

목차

Abstract
1. Introduction
2. Experimental
3. Results and Discussion
4. Conclusions
References

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UCI(KEPA) : I410-ECN-0101-2021-433-001480529