지원사업
학술연구/단체지원/교육 등 연구자 활동을 지속하도록 DBpia가 지원하고 있어요.
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논문 기본 정보
- 자료유형
- 학술저널
- 저자정보
- 발행연도
- 2015.8
- 수록면
- 197 - 201 (5page)
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초록· 키워드
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Liquid chromatographic enantiomer separation of α-amino acids and their methyl and ethyl esters as fluorenylmethoxycarbonyl (FMOC) derivatives was performed using a recently developed chiral column (Chiralpak IE) based on polysaccharide derivative under simultaneous UV detection and fluorescence detection. The degree of enantiomer separation of α-amino acid esters as FMOC derivatives is generally higher than that of the corresponding α-amino acids. Especially, α-amino acid methyl esters showed the greatest enantioseparation. As this method developed in this study can be applied to determine the chemical and optical purity of α-amino acids and esters, it is expected to be quite useful for their chiral separation using Chiralpak IE.
목차
Abstract
1. INTRODUCTION
2. MATERIALS AND METHOD
3. RESULTS AND DISCUSSION
4. CONCLUSION
REFERENCES
참고문헌 (18)
참고문헌 신청
[학술지(정기간행물)] - Yashima, E. / 2001 / Polysaccharide-based chiral stationary phases for high-performance liquid chromatographic enantioseparation / J. Chromatogr. A 906 : 105 ~ 125
[학술지(정기간행물)] - Chankvetadze, B. / 2012 / Recent developments on polysaccharidebased chiral stationary phases for liquid-phase separation of enantiomers / J. Chromatogr. A 1269 : 26 ~ 51
[기타자료] - Daicel Chemical Industries, Ltd / 2008 / Application Guide for Chiral HPLC selection
[학술지(정기간행물)] - Zhang, T. / 2005 / Solvent versatility of immobilized 3,5-dimethylphenylcarbamate of amylose in enantiomeric separations by HPLC / J. Chromatogr. A 1075 : 65 ~ 75
[학술지(정기간행물)] - Zhang, T. / 2006 / Cellulose 3,5-dimethylphenylcarbamate immobilized on silica: A new chiral stationary phase for the analysis of enantiomers / Anal. Chim. Acta 557 : 221 ~ 228
[학술지(정기간행물)] - Chankvetadze, B. / 2012 / Recent developments on polysaccharidebased chiral stationary phases for liquid-phase separation of enantiomers / J. Chromatogr. A 1269 : 26 ~ 51
[기타자료] - Daicel Chemical Industries, Ltd / 2008 / Application Guide for Chiral HPLC selection
[학술지(정기간행물)] - Zhang, T. / 2005 / Solvent versatility of immobilized 3,5-dimethylphenylcarbamate of amylose in enantiomeric separations by HPLC / J. Chromatogr. A 1075 : 65 ~ 75
[학술지(정기간행물)] - Zhang, T. / 2006 / Cellulose 3,5-dimethylphenylcarbamate immobilized on silica: A new chiral stationary phase for the analysis of enantiomers / Anal. Chim. Acta 557 : 221 ~ 228
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