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논문 기본 정보

자료유형
학위논문
저자정보

박수진 (영남대학교, 嶺南大學校)

지도교수
李載雄
발행연도
2019
저작권
영남대학교 논문은 저작권에 의해 보호받습니다.

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Abstract

In this study, cotton fabrics were coated with TiO2 nanoparticles using 3-mercaptopropyltrimethoxysilane(3-MPTMS), which is highly reactive to cotton fabrics, as a medium, and the characteristics, antimicrobial properties, and photodegradation properties of the fibers were measured. The manufacturing process is as follows. (1) 3-MPTMS was added to isopropanol, and TiO2 colloid was added to the mixture to prepare a solution. (2) Cellulose fibers were immersed in the prepared 3-MPTMS/TiO2 solution, stirred for 90minutes at 45℃ in a constant temperature water bath, and dried there after. In order to identify the morphology of the cellulose fibers coated with TiO2 nanoparticles, the surface was observed with a scanning electron microscope(SEM), and SEM-EDS was measured to identify the adhesion of TiO2 nanoparticles. The SEM images showed TiO2 nanoparticle and 3-MPTMS coated layers on the fibers and it was identified that TiO2 nanoparticles were attached to the cellulose fibers. The antimicrobial activity of 3-MPTMS/TiO2-treated cotton fabrics was measured using a bacterial reduction method. 3-MPTMS/TiO2 cellulose fibers which was irradiated by ultra violet light, showed antimicrobial activity against Escherichia coli (ATCC 43895) and Staphylococcus aureus (ATCCBAA-1707) unlike unirradiated fibers. The cellulose fibers were stained with methylene blue and the photodegradation performance of the stained fabrics was analyzed. The stained fabrics showed high degradation performance with photolytic reactions of TiO2 nanoparticles.

목차

1. 서론 1
1.1 연구배경 1
1.2 연구목적 4
2. 실험 및 방법 7
2.1 실험 재료 7
2.2 3-MPTMS 및 TiO2 나노입자 코팅 8
2.3 투과전자현미경 (TEM) 9
2.4 주사전자현미경 (SEM) 9
2.5 원자간력 현미경 (AFM) 10
2.6 광전자분광기 (XPS) 10
2.7 세탁견뢰도 테스트 11
2.8 항균성 테스트 11
2.9 광분해 특성 12
3. 결과 및 고찰 13
3.1 TiO2 colloid 특성 분석 13
3.2 TiO2 나노입자가 부착된 셀룰로오스 표면 및 원소 분석 15
3.3 처리 조건에 따른 TiO2 나노입자의 부착량 분석 23
3.4 세탁견뢰도 및 내구성 테스트 29
3.5 항균성 테스트 31
3.6 광분해 특성 33
4. 결론 35
참고문헌 36
Abstract 44

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