지원사업
학술연구/단체지원/교육 등 연구자 활동을 지속하도록 DBpia가 지원하고 있어요.
커뮤니티
연구자들이 자신의 연구와 전문성을 널리 알리고, 새로운 협력의 기회를 만들 수 있는 네트워킹 공간이에요.
초록· 키워드
오류제보하기
Bisphenols and phthalates are endocrine-disrupting chemicals that are commonly used in packaging and as plasticizers. However, they pose health risks through ingestion, inhalation, and dermal contact. Accurate analysis of these pollutants is challenging owing to their low concentration and their presence in complex oil matrices. Therefore, they require efficient extraction and detection methods. In this study, an analytical method for the simultaneous quantification of bisphenols and phthalates in corn oil is developed. The dynamic multiple reaction monitoring mode of liquid chromatography-tandem mass spectrometry is used according to the different polarities of bisphenols and phthalates. The method is validated by assessing system suitability, linearity, accuracy, precision, homogeneity, and stability. The determination coefficients are higher than 0.99, which is acceptable. The percentage recovery and coefficient of variation of the accuracy and precision confirm that this analytical method is capable of simultaneously quantifying bisphenols and phthalates in corn oil. The bisphenols and phthalates in the formulations and pretreatment samples are stable for 7 d at room temperature and 24 h in an auto-sampler. Therefore, this validated analytical method is effective for the simultaneous quantification of bisphenols and phthalates in oils.
목차
Abstract
1. Introduction
2. Experimental
3. Results and Discussion
4. Conclusions
References
참고문헌 (20)
참고문헌 신청
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O. Ballesteros, A. Zafra, A. Navalón, and J. L. Vílchez, J. Chromatogr. A, 1121(2), 154-62 (2006). https://doi:10.1016/j.chroma.2006.04.014
H. T. Wan, P. Y. Leung, Y. G. Zhao, X. Wei, M. H. Wong, and Chris K. C. Wong, J. Hazard. Mater., 261, 763-769 (2013). http://dx.doi.org/10.1016/j.jhazmat.2013.01.034
R. Babu-Rajendran, G. Preethi, R. K. Poopal, N. P. Nikhil, K. Vimalkumar, A. Subramanian, and S. Krishna-Kumar, J. Chromatogr. B, 1079, 15-24 (2018). https://doi.org/10.1016/j.jchromb.2018.01.039
P. Viñas, N. Campillo, M. Pastor-Belda, A. Oller, and M. Hernández-Córdoba, J. Chromatogr. A, 1376, 18-25 (2015). http://dx.doi.org/10.1016/j.chroma.2014.12.012
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