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논문 기본 정보

자료유형
학술저널
저자정보
Vitalii Galkin (Korea Institute of Materials Science) Rambabu Kuchi (Korea Institute of Materials Science) Soon-Jae Kwon (Bucheon Techno Park) Tae-hoon Kim (Korea Institute of Materials Science) Jung-goo Lee (Korea Institute of Materials Science) Jong-Ryul Jeong (Chungnam National University) Dongsoo Kim (Korea Institute of Materials Science)
저널정보
한국자기학회 Journal of Magnetics Journal of Magnetics Vol.29 No.1
발행연도
2024.3
수록면
1 - 9 (9page)
DOI
10.4283/JMAG.2024.29.1.1

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초록· 키워드

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This paper reports the successful additive-free sintering of fine Nd-Fe-B powder prepared by reduction-diffusion (RD) and wet ball milling (WBM) washing. Fine Nd-Fe-B powder by RD poses difficulties in sintering without rare earth (RE) hydride additives due to oxidation or loss of the Nd-rich phase during the washing step. Here, the effect of different washing methods such as conventional water washing, acetic acid washing, and WBM washing on the Nd-rich phase and oxygen content of RD powders was examined. The WBM washing involves low energy milling in organic media, which simplifies the removal of impurities from the RD powder. Among all the samples, the magnet made by sintering with WBM powder showed the coercivity of 8.7 kOe and (BH)max of 33.7 MGOe, which are comparable to magnets made of acidic washed RD powder with the essential addition of NdHx of 10 wt% reported in other studies. This is considered that in the powder after WBM washing, oxygen content was decreased compared to water washing and Nd-rich phase remained compared to acidic washing, which resulted in successful densification during sintering and the formation of Ndrich areas in sintered body. This finding makes an important step towards the production of Nd-Fe-B based magnets from sintering with RD powder without additive.

목차

1. Introduction
2. Materials and Methods
3. Results and Discussion
4. Conclusions
References

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