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An electrochromic nickel oxide thin film was fabricated on a flexible PET/ITO substrate using a nanocrystallite-dispersed coating sol and bar coater. Nanocrystalline NiOx of 3-4 ㎚ crystallite size was first synthesized by base precipitation and thermal conversion. This NiO<SUB>x</SUB> nanocrystallite powder was mechanically dispersed in an alcoholic solvent mixed with a silane binder to prepare a coating sol for thin film. This sol method is different from the normal sol-gel method in that it does not require the conversion of precursor by heat treatment. Therefore, this method provides a very facile method to prepare NiO<SUB>x</SUB> thin films on any kind of substrate and it can be easily applied to mass production. The electrochromic performance of this NiO<SUB>x</SUB> thin film on PET/ITO electrode with a thickness of about 400 ㎚ was investigated in a nonaqueous LiClO4 electrolyte solution by cyclic voltammetric and repeated chronoamperometric measurements in conjunction with spectrophotometry. The visible light modulation of 44% and the colorization efficiency of 41 ㎠/C at 550 ㎚ were obtained at the step potentials of -0.8/+1.2 V vs Ag and a duration of 30 s.
목차
ABSTRACT
INTRODUCTION
EXPERIMENTAL
RESULTS AND DISCUSSION
CONCLUSION
REFERENCES
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