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Zn2+-doped CTAB@BiOCl inorganic–organic composites were prepared by a co-precipitation method with different aging periods. The results show that the aging period has great influence on the structure, morphology and surface area of Zn2+-doped CTAB@BiOCl. The as-synthesized samples tend to form lamellar stacking structure with the increase of the aging time. In addition, the surface area and pore size distribution of samples decrease with the aging period from 0 h to 48 h and then increase from 48 h to 96 h. Besides, the content of CTAB in these composites increases along with the aging period from 0 h to 3 h and then decreases from 3 h to 96 h. Their photocatalytic performances were evaluated by the degradation of Reactive Red 3 (X3B) under UV light irradiation. It is found that the photocatalytic performance of composites increases with the prolonging of the aging time, and 100 mg/L of X3B solution can be almost completely degraded within 16 min by S96. Moreover, the possible formation mechanism has been proposed and discussed in detail. The work can provide a new sight for broadening the application of co-precipitation in the preparation of nanomaterials and for in-situ one-step synthesis of inorganic– organic composites.
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