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논문 기본 정보
- 자료유형
- 학술저널
- 저자정보
- 저널정보
- 한국고분자학회 폴리머 폴리머 제45권 제4호
- 발행연도
- 2021.7
- 수록면
- 541 - 551 (11page)
- DOI
- 10.7317/pk.2021.45.4.541
이용수
초록· 키워드
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The dependence of structural and optical characteristics on the thermal annealing of a doped poly(4-phenylenediamine-co-2-aminophenol) nanostructured thin film [P4D2AP]<SUP>TF</SUP> as a doped polymer conductor nanostructured thin film was studied. [P4D2AP]<SUP>TF</SUP> was fabricated as a thin film (100 ± 2 ㎚) using the spin coating method. Various characterization methods for [P4A2AP]<SUP>TF</SUP> like Fourier-transform infrared spectroscopy (FTIR), ultraviolet-visible spectroscopic (UV-Vis), thermogravimetric analysis (TGA), and optical characteristics have been studied. The resulted X-ray diffraction (XRD) and scanning electron microscope (SEM) data have been employed to study interface composites. Density functional theory (DFT) was used for optimization by atomic orbital DFT code (DMol³) and Cambridge serial total energy package (CASTEP). Spectroscopic and structural characteristics for the thin film have confirmed the chemical composition and XRD observations revealed the same crystal structure. The fabricated film was annealed in the air for 1h at 100 and 200 ℃. XRD examination of [P4D2AP]<SUP>TF</SUP> displayed that symmetry is an orthorhombic with a space group (P<SUB>mcn</SUB>). The optical characteristics demonstrated that the thin film has a relatively high absorbance of 95%. The calculated energy gaps are 2.523 eV and 2.504 eV for DFT and experimental, respectively. In addition, the optoelectrical parameters of the film have been calculated for absorption index (k(λ)), refractive index (n(λ)), dielectric constant, and optical conductivity. CASTEP simulated values are consistent with the experimental values for optical parameters of [P4A2AP]<SUP>TF</SUP>. The findings of the structural and optical characteristics described the fabricated thin film can be utilized as a candidate material for optoelectronic devices and solar cells.
목차
Abstract
Introduction
Experimental
Results and Discussion
Conclusion
References
참고문헌 (41)
참고문헌 신청
Sherman, B. C.; Euler, W. B.; Force, R. R. The Modern Student Laboratory: Polyaniline-A Conducting Polymer: Electrochemical Synthesis and Electrochromic Properties. J. Chem. Ed. 1994, 71, A94.
Nalwa, H. S. Handbook of Advanced Electronic and Photonic Materials and Devices, Ten-Volume Set, Academic Press 2000.
Panah, N. B.; Mahjani, M. G.; Jafarian, M. Correlation between Irregular Surface Geometry and Certain Electrochemical Quantities in Poly-ortho-aminophenol. Prog. Org. Coat. 2009, 64, 33-38.
Wang, C. Y.; Mottaghitalab, V.; Too, C. O.; Spinks, G. M.; Wallace, G. G. Polyaniline and Polyaniline-Carbon Nanotube Composite Fibres as Battery Materials in Ionic Liquid Electrolyte. J. Power Sources 2007, 163, 1105-1109.
Hu, H.; Ortíz-Aguilar, B. E.; Hechavarría, L. Effect of pH Value of Poly(ethylenimine)-H2SO4 Electrolyte on Electrochromic Response of Polyaniline Thin Films. Opt. Mater. 2007, 29, 579-584.
Nalwa, H. S. Handbook of Advanced Electronic and Photonic Materials and Devices, Ten-Volume Set, Academic Press 2000.
Panah, N. B.; Mahjani, M. G.; Jafarian, M. Correlation between Irregular Surface Geometry and Certain Electrochemical Quantities in Poly-ortho-aminophenol. Prog. Org. Coat. 2009, 64, 33-38.
Wang, C. Y.; Mottaghitalab, V.; Too, C. O.; Spinks, G. M.; Wallace, G. G. Polyaniline and Polyaniline-Carbon Nanotube Composite Fibres as Battery Materials in Ionic Liquid Electrolyte. J. Power Sources 2007, 163, 1105-1109.
Hu, H.; Ortíz-Aguilar, B. E.; Hechavarría, L. Effect of pH Value of Poly(ethylenimine)-H2SO4 Electrolyte on Electrochromic Response of Polyaniline Thin Films. Opt. Mater. 2007, 29, 579-584.
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