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In this study, 16 antibiotics were selected from among the top 30 veterinary antibiotics sold in South Korea in 2014, as well as from among the pharmaceuticals targeted by EPA method 1694, in order to review analytical methods for the detection of trace levels of antibiotics in environmental samples: surface water, soils, animal origin foods, and manures. LC-MS/MS was heavily used. In the chromatography for the detection of the selected antibiotics, the $C_{18}$ column was mostly used at the temperature of $30{\sim}40^{\circ}C$. Water and methanol/acetonitrile were commonly chosen as a nonpolar and a polar mobile phase, respectively. Gradient elution was applied to separate multiclass antibiotics. Volatile additives, such as formic acid, acetic acid, and ammonium acetate were mixed with the mobile phase to improve the ionization efficiency of analytes and the sensitivity in MS detection. Electrospray ionization (ESI) was widely used in the LC-MS/MS and positive ionization was preferred to determine the selected antibiotics. A protonated $[M+H]^+$ molecule was selected as a precursor ion, and its two transitions were analyzed, one for quantitative measurement and the other for confirmation. This study reviewed linearity of the calibration curve, recovery, repeatability, method detection limits (MDLs), and method quantification limits (MQLs) for each target compound used to validate the developed analytical methods.
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참고문헌 (74)
참고문헌 신청
Aguilera-Luiz, M. M. / 2012 / Multiclass Method for Fast Determination of Veterinary Drug Residues in Baby Food by Ultra-High-Performance Liquid Chromatography-Tandem Mass Spectrometry / Food Chemistry 132(4):2171~2180
Avisar, D. / 2010 / Sorption of Sulfonamides and Tetracyclines to Montmorillonite Clay / Water, Air, & Soil Pollution 209(1):439~450
Axys Analytical Services, Analytical Procedure for the Analysis of Pharmaceutical Compounds in Solid and Aqueous Samples by LC-MS/MS, Axys Analytical Services proprietary
Babic, S. / 2006 / Solid Phase Extraction and HPLC Determination of Veterinary Pharmaceuticals in Wastewater / Talanta 70(4):732~738
Behera, S. K. / 2011 / Occurrence and Removal of Antibiotics, Hormones and Several Other Pharmaceuticals in Wastewater Treatment Plants of the Largest Industrial City of Korea / Science of the Total Environment 409(20):4351~4360
Avisar, D. / 2010 / Sorption of Sulfonamides and Tetracyclines to Montmorillonite Clay / Water, Air, & Soil Pollution 209(1):439~450
Axys Analytical Services, Analytical Procedure for the Analysis of Pharmaceutical Compounds in Solid and Aqueous Samples by LC-MS/MS, Axys Analytical Services proprietary
Babic, S. / 2006 / Solid Phase Extraction and HPLC Determination of Veterinary Pharmaceuticals in Wastewater / Talanta 70(4):732~738
Behera, S. K. / 2011 / Occurrence and Removal of Antibiotics, Hormones and Several Other Pharmaceuticals in Wastewater Treatment Plants of the Largest Industrial City of Korea / Science of the Total Environment 409(20):4351~4360
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