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논문 기본 정보
- 자료유형
- 학술저널
- 저자정보
- 저널정보
- 대한약학회 Archives of pharmacal research : a publication of the Pharmaceutical Society of Korea Archives of pharmacal research : a publication of the Pharmaceutical Society of Korea 제31권 제8호
- 발행연도
- 2008.1
- 수록면
- 1,066 - 1,072 (7page)
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초록· 키워드
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An analytical CE method was developed for the enantiomeric purity determination of fluvastatin enantiomers. Fluvastatin enantiomers were separated on an uncoated fused silica with 100 mM-borate solution containing 30 mg/mL of (2-hydroxypropyl)-$\beta$-cyclodextrin (HP-$\beta$-CD) as running buffer and fenoprofen as an internal standard. The linearity was observed within a $400-700\;{\mu}g/mL$ concentration range ($r^2{\geq}0.995$) for both fluvastatin enantiomers. The repeatability expressed as coefficient of variation (CV) of the method were 0.96 and 0.92% for (+)-3R, 5S and (-)-3S, 5R-fluvastatin, respectively. The limit of detection and quantification for both fluvastatin enantiomers were $1.5\;{\mu}g/mL$ and $2.5\;{\mu}g/mL$, respectively.
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