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자료유형
학술저널
저자정보
Hem, Lina (Natural Products Chemistry Laboratory, Biotechnology Research Institute, Chonnam National University) El-Aty, A.M. Abd (Department of Pharmacology, Faculty of Veterinary Medicine, Cairo University) Park, Jong-Hyouk (Natural Products Chemistry Laboratory, Biotechnology Research Institute, Chonnam National University) Shim, Jae-Han (Natural Products Chemistry Laboratory, Biotechnology Research Institute, Chonnam National University)
저널정보
한국응용생명화학회 Applied Biological Chemistry Applied Biological Chemistry 제55권 제6호
발행연도
2012.1
수록면
765 - 768 (4page)

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This paper presents a simple and sensitive method for detection and quantification of neonicotinoids (dinotefurans) in pepper. Extraction of pesticide was carried out with acetonitrile and water partition, and passed through cleanup. The residue levels were determined by high performance liquid chromatography with UV detection and liquid chromatography-tandem mass spectrometry (LC-MS/MS) confirmation. The analytical method was very good within a wide range of concentrations with linearity ($r^2$) of 1.00. The recovery at two fortification levels ranged between 91.2 to 97.5% with relative standard deviation less than 6.0%. The method was successfully applied for determination of the analyte in pepper grown under greenhouse conditions.

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