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논문 기본 정보

자료유형
학술저널
저자정보
Kim, Sung-Woo (Biotechnology Research Institute, Chonnam National University) Abd El-Aty, A.M. (Biotechnology Research Institute, Chonnam National University) Choi, Jeong-Heui (Biotechnology Research Institute, Chonnam National University) Rahman, Md. Musfiqur (Biotechnology Research Institute, Chonnam National University) Hong, Su Myeong (Department of Agri-food Safety, National Academy Science, Rural Development Administration) Im, Geon-Jae (Department of Agri-food Safety, National Academy Science, Rural Development Administration) Shim, Jae-Han (Biotechnology Research Institute, Chonnam National University)
저널정보
한국응용생명화학회 Applied Biological Chemistry Applied Biological Chemistry 제57권 제6호
발행연도
2014.1
수록면
783 - 787 (5page)

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The present study estimated the residue levels of abamectin ($B_{1a}$) in green tea leaves and tea infusion. Samples were hydrated with water prior to extraction by using the quick, easy, cheap, effective, rugged, safe method and was analyzed with liquid chromatography-tandem mass spectrometry in positive ion mode. The matrix-matched calibration was linear over the concentration range of 0.01-2mg/kg with determination coefficients ($R^2$) >0.995. Recovery rates at two spiking levels (0.1 and 0.5 mg/kg) ranged between 80.5-99.7% with a relative standard deviation <11%. The compound was stable at $20^{\circ}C$ for 174 days with a recovery estimate of 109.9%. Although the maximum residue limit was not established by the Ministry of Food and Drug Safety, Republic of Korea, the limit of quantitation was very low at 0.01 mg/kg. The method was successfully applied to field incurred samples and detected residue of 0.02 mg/kg in green tea samples sprayed twice (7-3 days). Abamectin was not transferred to tea infusion.

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