지원사업
학술연구/단체지원/교육 등 연구자 활동을 지속하도록 DBpia가 지원하고 있어요.
커뮤니티
연구자들이 자신의 연구와 전문성을 널리 알리고, 새로운 협력의 기회를 만들 수 있는 네트워킹 공간이에요.
논문 기본 정보
- 자료유형
- 학술저널
- 저자정보
- 발행연도
- 2013.10
- 수록면
- 457 - 467 (11page)
이용수
초록· 키워드
오류제보하기
A quick and simple method for simultaneous determination of the 30 ginsenosides (ginsenoside Ro, Rb1, Rb2, Rc, Rd, Re, Rf, Rg1, 20(S)-Rg2, 20(R)-Rg2, 20(S)-Rg3, 20(R)-Rg3, 20(S)-Rh1, 20(S)-Rh2, 20(R)-Rh2, F1, F2, F4, Ra1, Rg6, Rh4, Rk3, Rg5, Rk1, Rb3, Rk2, Rh3, compound Y, compound K, and notoginsenoside R1) in Panax ginseng preparations was developed and validated by an ultra performance liquid chromatography photo diode array detector. The separation of the 30 ginsenosides was efficiently undertaken on the Acquity BEH C-18 column with gradient elution with phosphoric acids. Especially the chromatogram of the ginsenoside Ro was dramatically enhanced by adding phosphoric acid. Under optimized conditions, the detection limits were 0.4 to 1.7 mg/L and the calibration curves of the peak areas for the 30 ginsenosides were linear over three orders of magnitude with a correlation coefficients greater than 0.999. The accuracy of the method was tested by a recovery measurement of the spiked samples which yielded good results of 89% to 118%. From these overall results, the proposed method may be helpful in the development and quality of P. ginseng preparations because of its wide range of applications due to the simultaneous analysis of many kinds of ginsenosides.
목차
INTRODUCTION
MATERIALS AND METHODS
RESULTS AND DISCUSSION
REFERENCES
참고문헌 (33)
참고문헌 신청
1. [단행본] - Soldati F. / 2000 / Panax ginseng: standardization and biological activity, In Biologically active natural products / CRC press : 209 ~ 232
2. [학술지(정기간행물)] - Christensen LP. / 2009 / Ginsenosides chemistry, biosynthesis, analysis, and potential health effects / Adv Food Nutr Res 55 : 1 ~ 99
3. [학술지(정기간행물)] - Fuzzati N. / 2004 / Analysis methods of ginsenosides / J Chromatogr B Analyt Technol Biomed Life Sci 812 : 119 ~ 133
4. [학술지(정기간행물)] - Oleszek WA. / 2002 / Chromatographic determination of plant saponins / J Chromatogr A 967 : 147 ~ 162
5. [학술지(정기간행물)] - Oleszek W / 2006 / Chromatographic determination of plant saponins: an update (2002-2005) / J Chromatogr A 1112 : 78 ~ 91
2. [학술지(정기간행물)] - Christensen LP. / 2009 / Ginsenosides chemistry, biosynthesis, analysis, and potential health effects / Adv Food Nutr Res 55 : 1 ~ 99
3. [학술지(정기간행물)] - Fuzzati N. / 2004 / Analysis methods of ginsenosides / J Chromatogr B Analyt Technol Biomed Life Sci 812 : 119 ~ 133
4. [학술지(정기간행물)] - Oleszek WA. / 2002 / Chromatographic determination of plant saponins / J Chromatogr A 967 : 147 ~ 162
5. [학술지(정기간행물)] - Oleszek W / 2006 / Chromatographic determination of plant saponins: an update (2002-2005) / J Chromatogr A 1112 : 78 ~ 91
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UCI(KEPA) : I410-ECN-0101-2014-520-002777951